C2.1.1.1 Quantitative Determination of Carbon

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Quantitative Determination of Carbon

In experiment C2.1.1.1, the carbon content of an organic compound is determined quantitatively. In a combustion analysis, the substance is passed over glowing copper(II) oxide at approx. 800 °C – 900 °C. The carbon is converted to CO2 and the hydrogen is converted to H2O. The CO2 gas generated is collected in a gas syringe and the volume is measured.

Components of experiment:

1 664 069 Reaction tube, quartz, 220 x 25 mm Ø, for butane combustion
2 665 374 Drying tube, 1 GL 18 and 1 GL 25, 120 mm x 30 mm diam.
2 665 914 Gas syringe, 100 ml with 3-way stopcock
1 656 017 Teclu burner, universal
1 666 724 Wide-flame attachment
1 666 729 Safety gas hose, 1 m
1 666 603 Base rail, 95 cm
4 666 609 Stand tube, 45 cm, Ø 10 mm
4 666 615 Universal bosshead
5 301 09 Bosshead S
4 666 555 Universal clamp, 0…80 mm
1 301 72 Universal clamp, 0…120 mm
1 666 962 Double-ended spatula, stainless steel, 150 mm
1 665 994 Graduated pipette, 1 ml
1 666 003 Pipetting ball (Peleus ball)
1 667 180 Rubber tubing, 1 m x 7 mm diam., DIN 12865
1 604 481 Rubber tubing, 1 m x 4 mm diam., DIN 12865
1 665 004 Funnel, Boro 3.3, 80 mm diam.
1 604 510 Tubing connector, 4…15 mm
1 661 000 Minican pressurised gas canister, nitrogen
1 660 989 Minican pressurised gas canister, n-Butane
1 660 980 Fine regulating valve for minican gas canisters
1 667 034 Tweezers, blunt, 200 mm
1 672 9410 Copper oxide, wire form, 250 g
1 671 2410 Calcium chloride, granulated, 250 g
1 674 4310 1-Propanol, 250 ml
1 672 1010 Glass wool, 100 g

Experiment Instructions Click HERE

 

 

Additional information

Weight 85 lbs
Dimensions 48 × 48 × 36 in
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